Synthesis And Subsequent Low Temperature, Electrochemical Crystal Growth Of Bis-(Tetramethyltetraselenafulvalenium) Periodate, (TMTSF)2IO4

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Kuhr, Christian

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1984-04-01

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thesis

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Tetrabutylammonium periodate, synthesized from tetrabutylammonium hydrogensulfate and sodium periodate, is found to produce high geometric quality crystals, upon electrochemical oxidation with tetramethyltetraselenafulvalene These crystals are currently undergoing x-ray diffraction studies to determine the crystal structure, and possibility of superconducting properties.

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